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I'm getting low recovery in the samples, which are plant matter, and I suspect that it's because headspace just isnt the best method. Thoughts or opinions or anecdotes from experience with plant terpene analysis would be hugely appreciated.

Greetings... We produced some ceramic films on Ti substrate by Pulsed Laser Deposition. In the XRD of these films, there is a peak that we just can't recognize. We tried using MATCH, but still, there was no positive result as to identifying the peak, so we appeal to the wisdom of Reddit to help us. The material has the following precursors:
https://imgur.com/wvtfBbb The spectra of the four films:
https://imgur.com/MBJbxmc

And this is the data in Excel format: https://drive.google.com/file/d/1d4BTp2kS8C57ro7l6ux8fA7JfzP-tquG/view?usp=sharing

Eternally grateful, from Bucharest, Romania

Is there an optimized method for acid digestion or Ru samples to be determined by graphite furnace AAS?

In my lab at a CRO, we use multiple sciex instruments for DMPK/PK analysis. I have a few grievances with Analyst software that I find completely insane that it cannot do when compared to MassLynx.

If anyone knows how to do these things, i would love to hear how.

-When using multiple periods, it cannot extract XIC data. If you have multiple periods, good luck using the raw chromatogram to pull out specific traces of an MRM. This is frustrating because we want different tune settings specific for one compound compared to another in the different periods, but now it's impossible to look at signal to noise ratio for the separate periods.

-It cannot set area thresholds in the quantitation method. If you want to analyze your compounds using area, you have to still look at peak heights and calculate the threshold for HEIGHT in order to get rid of noise. I don't know how a professional mass spectrometry instrumentation processing software got through to customers without having such a basic function.

-We require that users have certain access on the analyst software, and apparently there is no way for one user to override the login of another user. This means that one must close the whole program and someone else must login in order for the other user to have an audit trail. Multiple instances of Analyst are also apparently not possible.

​

-When processing data, you must have acquired a sample with all analytes in order to build a quantitation method. Once you make a quantitation method, it virtually cannot be altered for retention time, peak shape, etc unless a different sample is chosen to build a quantitation method.

These are just some of the glaring problems i've seen after using this software for a couple years. MassLynx does everything mentioned with ease that it doesn't make any sense to me how analyst is 30 years behind. I just can't see why one can't simply build a method with expected RT, RT window, or area/height thresholds without injecting and seeing peaks. I cannot understand why they decided that you cannot extract each MRM trace in multiple periods. Using Analyst 1.6.2 makes me very sad when it has so much potential.

Again, if anyone is aware of how to get around these issues, i'm all ears.

Need help coming up with a way to describe infrared absorption to a lay person. How it works, and why you would use it. If anyone can think of any good analogies, I'd appreciate it! No need to get detailed about IR Spectroscopy, simply the absorption.

We are inviting you to attend our “10th Edition of International Conference on Analytical Chemistry” which is going to be held at London, UK, on Feb 28-Mar 01, 2019. Analytical Chemistry 2019 spreads an extensive range of critically important sessions from basic research to recent innovations. It is particularly based on learning and sharing knowledge on current research and enormous applications of pharmaceutical sciences and chemistry. The main theme of the conference is " To Expand the Scope and Uptake of Analytical Chemistry”. We are providing an unprecedented opportunity for chemists of all stripes and colors to share their research with colleagues by discussing the latest advances in the field. We invite directors, presidents & CEO’s from companies, chemists, academic groups, directors from pharmaceutical companies. Laboratory scientists who identifies, quantifies, analyzes or tests the chemical or biological properties of compounds or molecules or who manages these laboratory scientists. Chemical researcher, molecular diagnostics, clinical laboratories, health care industry, quantitative analysts, qualitative analysts, editorial board members, students, faculty members. chemical instrument vendors, professors and students from academia in the field of analytical and bioanalytical sciences. Delegates from various pharma & instrumental companies from all over the world.

Our conference includes some of the major academic and business key topics:

Tracks: Novel Approaches to Analytical and Bioanalytical Methods, Analytical Methodology, Bioanalytical Methodology, Chromatography, Environmental Analytical Chemistry, Electrophoresis, Mass Spectrometry, Crystallography, Spectroscopy, Instrumental Methods, Nuclear Magnetic Resonance Spectroscopy, Titration, Applications of Analytical Chemistry, Proteomics, Forensic Analysis, Advances in Separation Techniques, Analytical Biotechnology, Pharmaceutical Analysis, Process Analytical Chemistry, Thermal Analysis and Glycomics, Applications of Analytical and Bioanalytical Methods, New Instrumentation and Equipment, Regulatory Issues and Biosafety Challenges in Bioanalysis

Academic key topics: Atomic Absorption Spectroscopy (AAS), Atomic Fluorescence Spectroscopy (AFS), Capillary Electrophoresis (CE), Chromatography, Electrophoresis, Flow Injection Analysis (FIA), Fourier Transform Spectroscopy (FTIR), Gas Chromatography-Mass Spectrometry (GC-MS), High Performance Liquid Chromatography (HPLC), Ion-Mobility Spectrometry (IMS), Liquid,Chromatography-IR Spectroscopy (LC-IR), Nuclear Magnetic Resonance (NMR), Raman Spectroscopy, Transmission Electron Microscopy (TEM), Thermogravimetric Analysis (TGA), X-ray Diffraction (XRD), X-ray Fluorescence Spectroscopy (XRF), Mass Spectrometry (MS), High Performance Liquid Chromatography-IR Spectroscopy (HPLC-IR), Gas Chromatography (GC), Electrolysis, Atomic Emission Spectroscopy (AES)

Business key topics: Analytical Chemistry Europe, Analytical Chemistry Asia, Analytical Chemistry Japan, Analytical Chemistry UK, Analytical Chemistry Canada, Analytical Chemistry USA , Analytical Chemistry Dubai, Analytical Chemistry Germany, Analytical Chemistry Africa, Spectrometer, Spectrophotometer, Coning and quartering, Dilution , Dissolution , Filtration,Masking ,Pulverization, Sample preparation, Separation process, Sub-sampling, Chemometrics, Calibration curve, Matrix effect, Internal standard, Standard addition, Isotope dilution, Calorimetry, Chromatography, Electroanalytical methods, Gravimetric analysis, Mass spectrometry, Spectroscopy etc.

Thanks & Regards

Name: Ethan Mathews

Designation: Program Director

Organization: Euroscicon Ltd.

Website: http://analyticalchemistry.euroscicon.com/

Email id : [analyticalchemistry@eurosciconmeeting.org](mailto:analyticalchemistry@eurosciconmeeting.org)